Wiggens BR Series- High Pressure Reactor ( Stainless steel reactor)

Description

These high-pressure reactors fit best for tests with source materials that are rather expensive or complicated to produce. Both BR-25 and BR-40 are available in stainless steel and Hastelloy.
Additionally, they can be equipped with TFMTM-PTFE inserts. The volume of the reactor vessels depends on the specification chosen and may vary from 30 ml up to 68 ml.
The BR 25/40 high-pressure reactor is notable for its ease of use. To seal the reactor, the vessel is simply screwed into the lid by hand. The reactor is sealed using a conical flange connection and O-ring seal of PTFE, FKM, or FFKM. The appropriate fitting inserts are available in stainless steel 1.4571 (SUS 316LTI) or Hastelloy C-22. A total of 6 connection options are provided in the lid, which can be selected from the following:
*  Immersion tube for temperature probes
*  Rupture disc of metal for the safe limitation of maximum pressure
*  Pressure display
*  Vent valve
*  2 freely selectable, for example for a gas sampling valve or liquid sampling point
Temperature is regulated using a temperature probe that detects the inner temperature of the reactor in an immersion tube. A second temperature probe can optionally be used as an independent overheating safety.

Features
*  The Powerful Mini-Reactor: For valuable reagents
*  25 or 40ml / 200 bar / 300℃ (PTFE-Lined 230° )
*  Threaded closure; to be operated manually without tools
*  O-seal ring made of Viton®, PTFE or Kalrez®
*  Either with PTFE-insert or completely made of SUS 316LTl or Hastelloy®
*  Heating and stirring by laboratory hot-plate with an integrated magnetic stirrer
*  Optionally 2’nd thermocouple

Technical Specification

		BR-25
Material		SUS316Ti or HC	SUS316Ti + PTFE
Temperature max.		300℃	230℃
Pressure max.		200 bar	200 bar
Reactor Vessel	Volume	approx. 30 ml	approx. 47 ml
	Inner Diameter	25 mm	27 mm
	Inner Height	62 mm	83 mm
	Weight	approx. 0.6 kg
TFMTM-PTFE Insert (optional)	Volume	–	approx. 29 ml*
	Inner Diameter	–	22 mm*
	Inner Height	–	77 mm*
Armatures	Standard Armatures	Rupture Disc, Dip Tube, Valve
	Pressure Measurement	analog and/or digital
	Ports (total)	6	6
	Ports (free)	2**	2**
	Type of connection	1/8″ Tube Connection	1/8″ Tube Connection
Heating Systems (optional)	Electrical Heating mantle	CHM-25	CHM-25
	Julabo thermostat	CTM-25	CTM-25
Stirring	Magnetic stirrer	BLH-800 / 801	BLH-800 / 801
Stand	Stand for BR-25 lid

* In this specification only to use with PTFE Insert
* The number of free ports can be enlarged by the use of T-connections

This high-pressure reactor is attractive due to its many stirring and heating variants. It is available in stainless steel 1.4571 (SUS 316LTI), Hastelloy C-22, or with PTFE lining on all sides. The usable volume of the reactor can be varied between 310 ml and 600 ml using different reactor vessels.
The BR-300/500 high-pressure reactor is notable for its ease of handling. The reactor is closed using a manual quick closure that can be attached without the use of tools. The reactor seal is established using a conical flange lock and O-ring seal of PTFE, FKM, or FFKM. The appropriate fitting inserts are available in stainless steel 1.4571 (SUS 316LTI) or Hastelloy C-22. A total of 6 connection options are provided in the lid, which can be selected from the following:
*  Immersion tube for the temperature probe
*  Rupture disc of metal for safe limitation of the maximum pressure
*  Pressure display 1 vent valve
*  Vent valve
*  2 freely configurable fittings, for example for a gas sampling
Temperature is regulated using a temperature probe that detects the inner temperature of the reactor in an immersion tube. A second temperature probe can optionally be used as an independent overheating safety.

Features
*  300, 350, 500, 600ml / 200 bar / 300℃ (PTFE-Lined 230° )
*  Quick closure ring, to be operated manually without tools
*  O-seal ring made of Viton®, PTFE or Kalrez®
*  Either with PTFE-insert or completely made of SUS 316LTl or Hastelloy®
*  Heating and stirring by laboratory hot-plate with an integrated magnetic stirrer (only 300-350ml)
*  Heating by electrical or thermostated mantle
*  Stirring by magnetic clutch and separate drive
*  Optionally internal heating/cooling coil
*  Optionally 2’nd thermocouple

Technical Specification BR-300

		BR-300
Material		SUS316Ti or HC	SUS316Ti + PTFE
Temperature max.		300℃	230℃
Pressure max.		200 bar
Reactor Vessel	Volume	approx. 390 ml
	Inner Diameter	68 mm
	Inner Height	108 mm
	Weight	approx. 4 kg
TFMTM-PTFE Insert* (integrated)	Volume	–	approx. 310 ml
	Inner Diameter	–	62.5 mm
	Inner Height	–	98 mm
Armatures	Standard Armatures	Rupture Disc, Dip Tube, Valve, Tool
	Pressure Measurement	analog and/or digital
	Ports (total)	6
	Ports (free)	2**
	Type of connection	8 mm Tube Connection
Heating Systems (optional)	Electrical Heating mantle	CHM-300
	Julabo thermostat	CTM-300
	Heating Coil	√
Stirring	Magnetic stirrer	BLH-800 / 801
	Overhead stirrer with magnetic clutch	WB20C and RV 100-SS
Stand	Pneumatic bench-top stand (with overhead stirrer) Stand for BR-300 lid (with a magnetic stirrer)

* When using PTFE inserts the maximum allowable temperature is 230℃
* The number of free ports can be enlarged by the use of T-connections

 

This high-pressure reactor is ideally suitable for larger experimental runs. This high-pressure reactor is available in stainless steel 1.4571 (SUS 316LTI), Hastelloy C-22, or with PTFE lining on all sides. The usable volume of the reactor can be varied between 1,000 ml and 2,240 ml using different reactor vessels.
The BR 1000/1500/2000 high-pressure reactor is notable for its ease of handling. The reactor is closed using a manual quick closure that can be attached without the use of tools. The reactor seal is established using a conical flange lock and O-ring seal of PTFE, FKM, or FFKM. The appropriate fitting inserts are available in stainless steel 1.4571 (SUS 316LTI) or Hastelloy C-22. A total of 6 connection options are provided in the lid, which can be selected from the following:
* Immersion tube for temperature probes
* Rupture disc of metal for the safe limitation of maximum pressure
* Pressure display
* Vent valve
* 2 freely selectable fittings, for example for a gas sampling valve or liquid sampling point
Temperature is regulated using a temperature probe that detects the inner temperature of the reactor in an immersion tube. A second temperature probe can optionally be used as an independent overheating safety. Appropriate stand systems are available.

Features
* 1000, 1500, 1700, 2000 or 2300 ml / 200 bar / 300℃ (PTFE-Lined 230° )
* Quick closure chain, to be operated manually without tools
* O-seal ring made of Viton®, PTFE or Kalrez®
* Either with PTFE-insert or completely made of SUS 316LTi or Hastelloy®
* Heating by electrical or thermostated mantle
* Stirring by magnetic clutch and separate drive
* Optionally internal heating/cooling coil
* Optionally 2’nd thermocouple

Technical Specification

		BR-1000
Material		SUS316Ti or HC	SUS316Ti + PTFE
Temperature max.		300℃	230℃
Pressure max.		200 bar
Reactor Vessel	Volume	approx. 1,220 ml
	Inner Diameter	90 mm
	Inner Height	193 mm
	Weight	approx. 10.5 kg
TFMTM-PTFE Insert* (integrated)	Volume	–	approx. 1,000 ml
	Inner Diameter	–	84 mm
	Inner Height	–	182.5 mm
Armatures	Standard Armatures	Rupture Disc, Dip Tube, Valve, Tool
	Pressure Measurement	analog and/or digital
	Ports (total)	6
	Ports (free)	2**
	Type of connection	8 mm Tube Connection
Heating Systems (optional)	Electrical Heating mantle	CHM-1000
	Julabo thermostat	CTM-1000
	Heating Coil	√
Stirring	Overhead stirrer with magnetic clutch	WB20C and RV 100-SS
Stand		Electric lifting stand for BR-1000

* When using PTFE inserts the maximum allowable temperature is 230℃
* The number of free ports can be enlarged by the use of T-connections